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Ethyl nitroacetate

Product Name:
Ethyl nitroacetate
CAS No.
626-35-7
Chemical Name:
Ethyl nitroacetate
CBNumber:
CB1175310
Molecular Formula:
C4H7NO4
Formula Weight:
133.1
MOL File:
626-35-7.mol
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Ethyl nitroacetate Property

Boiling point:
105-107 °C25 mm Hg(lit.)
Density 
1.199 g/mL at 25 °C(lit.)
refractive index 
n20/D 1.424(lit.)
Flash point:
198 °F
storage temp. 
Keep Cold
pka
pK1:5.85 (25°C)
form 
Liquid
color 
Clear colorless to slightly yellow
Water Solubility 
Slightly soluble in water. Soluble in chloroform and ethyl acetate.
BRN 
1210027
InChIKey
FTKASJMIPSSXBP-UHFFFAOYSA-N
CAS DataBase Reference
626-35-7(CAS DataBase Reference)
NIST Chemistry Reference
Acetic acid, nitro-, ethyl ester(626-35-7)
EPA Substance Registry System
Acetic acid, nitro-, ethyl ester (626-35-7)
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Safety

Hazard Codes 
Xi
Risk Statements 
38
Safety Statements 
23-24/25-37
WGK Germany 
2
RTECS 
AJ1074000
Hazard Note 
Irritant
TSCA 
T
HazardClass 
IRRITANT, KEEP COLD
HS Code 
29159080
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N-Bromosuccinimide Price More Price(8)

Sigma-Aldrich Gold
Product number:
192333
Product name :
Ethyl nitroacetate
Purity:
97%
Packaging:
5g
Price:
$59
Updated:
2020/08/18
Buy:
Buy
Sigma-Aldrich Gold
Product number:
192333
Product name :
Ethyl nitroacetate
Purity:
97%
Packaging:
25g
Price:
$190
Updated:
2020/08/18
Buy:
Buy
TCI Chemical Gold
Product number:
N0657
Product name :
Ethyl Nitroacetate
Purity:
>95.0%(GC)
Packaging:
5g
Price:
$47
Updated:
2020/06/24
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Buy
TCI Chemical Gold
Product number:
N0657
Product name :
Ethyl Nitroacetate
Purity:
>95.0%(GC)
Packaging:
25g
Price:
$140
Updated:
2020/06/24
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Buy
Alfa Aesar Gold
Product number:
A14433
Product name :
Ethyl nitroacetate, 97%
Packaging:
1g
Price:
$18.8
Updated:
2020/06/24
Buy:
Buy
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Ethyl nitroacetate Chemical Properties,Usage,Production

Chemical Properties

clear colourless to slightly yellow liquid

Uses

Ethyl Nitroacetate is an ester of nitrocarboxylic acid used as an intermediate in the preparation of unsubstituted amino acids.

Synthesis Reference(s)

The Journal of Organic Chemistry, 59, p. 1208, 1994 DOI: 10.1021/jo00084a047

Purification Methods

Purify the ester by repeated distillation. IR:max 1748 (CO2), 1570 and 1337 (NO2), and 800cm-1 [Haszeldine J Chem Soc 2525 1953]. The hydrazine salt crystallises from 95% EtOH or MeOH as yellow crystals m 104-105o [Ungnade & Kissinger J Org Chem 22 1661 1957, Emmons & Freeman J Am Chem Soc 77 4391 1955]. [Beilstein 2 IV 537.]

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Ethyl nitroacetate Suppliers

Global(212)Suppliers
Henan Jiuhua Biological Technology Co., Ltd.
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Alfa Aesar
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