ChemicalBook > CAS DataBase List > ISOCYANOBENZENE
ISOCYANOBENZENE
- Product Name:
- ISOCYANOBENZENE
- CAS No.
- 931-54-4
- Chemical Name:
- ISOCYANOBENZENE
- CBNumber:
- CB3382268
- Molecular Formula:
- C7H5N
- Formula Weight:
- 103.12
- MOL File:
- 931-54-4.mol
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ISOCYANOBENZENE Property
- Boiling point:
- 183.35°C (rough estimate)
- Density
- 1.0248 (rough estimate)
- refractive index
- 1.6760 (estimate)
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Safety
- Risk Statements
- 20/21/22
- Safety Statements
- 26-36/37/39
- RIDADR
- UN 1672 6.1/ PGI
- HazardClass
- 6.1
- PackingGroup
- I
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ISOCYANOBENZENE Chemical Properties,Usage,Production
Preparation
To a flask containing 7.9 gm (0.33 mole) of sodium hydride in 100 ml of tetrahydrofuran is slowly added a mixture of 9.3 gm (0.1 mole) of aniline and 25.3 gm (0.10 mole) of bromoform. After the addition, the reaction is stirred for 1-2 hr at room temperature, and water is added (100 ml) dropwise. Ether (200 ml) is added and the ether layer washed four times with 50-ml portions of water, three times with 20-ml portions of dilute hydrochloric acid, and then with water. The resulting ether layer is dried over sodium sulfate, concentrated, and the residue distilled to afford 4.7 gm (45%), b.p. 52-53°C (13 mm Hg).
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931-54-4, ISOCYANOBENZENERelated Search:
1,2-DICHLORO-4-ISOCYANOBENZENE
Benzene, 1-isocyano-4-nitro- (9CI)
Phenyl isocyanide, 5-chloro-2-methoxy- (7CI, 8CI)
2-ISOCYANO-5-CHLOROBENZOTRIFLUORIDE
1,4-DIISOCYANOBENZENE
2-CYANOPHENYL ISOCYANIDE
2,5-DIMETHOXY-4-NITRO-PHENYLISOCYANIDE
2-METHOXY-5-NITRO-PHENYLISOCYANIDE
4-ETHYLPHENYL ISOCYANIDE
Benzonitrile, 4-isocyano- (9CI)
2-METHOXY-4-NITROPHENYL ISOCYANIDE
1,2-DICHLORO-3-ISOCYANOBENZENE
1,3-DICHLORO-5-ISOCYANOBENZENE
Benzene, 1-isocyano-3-nitro- (9CI)
Benzene, 1-isocyano-2-(trifluoromethyl)- (9CI)
4-METHYL-3-NITRO-PHENYLISOCYANIDE
1,1'-Methylenebis(4-isocyanobenzene)
2,6-DIMETHYLPHENYL ISOCYANIDE
- PHENYLISOCYANIDE
- Phenyl isonitrile
- Phenyl carbylamine
- ISOCYANOBENZENE
- 1-ISOCYANOBENZENE
- Benzoisonitrile
- Benzene, isocyano-
- PHENYL ISOCYANIDE (1-ISOCYANOBENZENE)
- 931-54-4
- C6H5NC