ChemicalBook > CAS DataBase List > 2-HYDROXY-5-METHYLBENZOPHENONE

2-HYDROXY-5-METHYLBENZOPHENONE

Product Name:
2-HYDROXY-5-METHYLBENZOPHENONE
CAS No.
1470-57-1
Chemical Name:
2-HYDROXY-5-METHYLBENZOPHENONE
CBNumber:
CB6306465
Molecular Formula:
C14H12O2
Formula Weight:
212.24
MOL File:
1470-57-1.mol
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2-HYDROXY-5-METHYLBENZOPHENONE Property

Melting point:
83-85 °C(lit.)
Boiling point:
312.08°C (rough estimate)
Density 
1.1035 (rough estimate)
refractive index 
1.6000 (estimate)
pka
8.24±0.43(Predicted)
CAS DataBase Reference
1470-57-1(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39
WGK Germany 
3
Hazard Note 
Irritant
HS Code 
29145000
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N-Bromosuccinimide Price More Price(3)

Sigma-Aldrich Gold
Product number:
H38608
Product name :
2-Hydroxy-5-methylbenzophenone
Purity:
99%
Packaging:
5g
Price:
$82.2
Updated:
2020/08/18
Buy:
Buy
TCI Chemical Gold
Product number:
H1008
Product name :
2-Hydroxy-5-methylbenzophenone
Purity:
>97.0%(GC)
Packaging:
5g
Price:
$89
Updated:
2020/06/24
Buy:
Buy
TCI Chemical Gold
Product number:
H1008
Product name :
2-Hydroxy-5-methylbenzophenone
Purity:
>97.0%(GC)
Packaging:
25g
Price:
$269
Updated:
2020/06/24
Buy:
Buy
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2-HYDROXY-5-METHYLBENZOPHENONE Chemical Properties,Usage,Production

Chemical Properties

yellow crystalline powder

Preparation

Preparation by condensation of benzotrichloride with p-cresol,
? in the presence of aluminium chloride in carbon disulfide for 2 h (75%). The 6,12-diphenyl-2,8-dimethyl-6,12-epoxy-6H,12H-dibenzo[b,f] dioxocin, an intermediate compound, was also formed under these conditions (29%). This “dioxocin”, by hydrolysis with concentrated sulfuric acid at r.t., gave the expected ketone (91%);
? in the presence of aqueous sodium hydroxide in a water bath for 4 h (33%) or in 32–40% aqueous sodium hydroxide at 70–80° (67%).

Synthesis Reference(s)

The Journal of Organic Chemistry, 38, p. 1924, 1973 DOI: 10.1021/jo00950a030

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2-HYDROXY-5-METHYLBENZOPHENONE Suppliers

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1470-57-1, 2-HYDROXY-5-METHYLBENZOPHENONERelated Search:

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