ciclonicate

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ciclonicate Basic information

Product Name:
ciclonicate
CAS:
53449-58-4
MF:
C15H21NO2
MW:
247.33
EINECS:
258-561-4
Mol File:
53449-58-4.mol
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ciclonicate Chemical Properties

Boiling point:
bp0.6 127-128°
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ciclonicate Usage And Synthesis

Originator

Bled, Poli, Italy ,1978

Manufacturing Process

To a solution of 142 g (1 mol) of trans-3,3,5-trimethylcyclohexanol in 400 cc of anhydrous benzene heated to 70 C is added gradually 178 g (1 mol) of niacin chloride hydrochloride. Heating is carried out under reflux conditions for 3 hours, the solution is cooled, the ester hydrochloride is filtered off and then recrystallized in an ethanol-ethyl ether mixture to obtain 227 g (80% yield) of product melting at 155°C to 157°C.
By treating the hydrochloride with an aqueous solution of NaOH at 0°C, the free base is obtained in the form of a viscous white liquid which boils at 115°C under 0.05 mm.

Therapeutic Function

Vasodilator

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ciclonicate (53449-58-4)Related Product Information

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ciclonicate SupplierMore

Leancare Ltd.
Tel:
+33 962096793
Email:
enquiry@leancare.co.uk
Lanospharma Laboratories Co.,Ltd
Tel:
13440048448
Email:
sales@lanospharma.com
2A PharmaChem USA
Tel:
(630) 737-0988
Email:
sales@2apharmachem.com
3B Scientific Corporation
Tel:
847.281.9822
Email:
sales@3bsc.com
Basic information Safety Related Supplier