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Phenylsulfenylchloride

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Phenylsulfenylchloride Basic information

Product Name:
Phenylsulfenylchloride
CAS:
931-59-9
MF:
C6H5ClS
MW:
144.6219
EINECS:
632-987-4
Mol File:
931-59-9.mol
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Phenylsulfenylchloride Chemical Properties

Boiling point:
262℃
Density 
1.25
Flash point:
110℃
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Phenylsulfenylchloride Usage And Synthesis

Preparation

To a flask containing 32.7 gm (0.15 mole) of diphenyl disulfide dissolved in 100 ml of dichloromethane containing 3 ml of pyridine is slowly dropwise added at room temperature 20.3 gm (0.15 mole) of freshly distilled sulfuryl chloride. After completion of the addition, the solution is stirred for an additional hour, concentrated under reduced pressure (12 mm Hg) at 25°C, and the residue distilled to afford 33 gm (76%), b.p. 49°C (4 mm Hg), of a dark red liquid.
Preparation of Benzenesulfenyl Chloride

Phenylsulfenylchloride Preparation Products And Raw materials

Raw materials

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Phenylsulfenylchloride(931-59-9)Related Product Information

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Beijing Donghualituo Techonlogy Development Co.,Ltd. Gold
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