5BETA-CHOLANIC ACID

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5BETA-CHOLANIC ACID Basic information

Product Name:
5BETA-CHOLANIC ACID
CAS:
546-18-9
MF:
C24H40O2
MW:
360.57
Mol File:
546-18-9.mol
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5BETA-CHOLANIC ACID Chemical Properties

Melting point:
150 °C
Boiling point:
473.6±13.0 °C(Predicted)
Density 
1.018±0.06 g/cm3(Predicted)
pka
4.76±0.10(Predicted)
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Safety Information

WGK Germany 
3
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5BETA-CHOLANIC ACID Usage And Synthesis

Purification Methods

Crystallise 5-cholanic acid from EtOH, Me2CO or AcOH. The ethyl ester has m 93-94o (from 80% EtOH), b 273o/12mm, [] D 20 +21o (CHCl3), and the methyl ester has m 86-87o (from MeOH) after purification through Al2O3 and eluting with *C6H6, and [] D 20 +21.2o (CHCl3). The 1H NMR (CDCl3) for the C18 & C19 protons has at 0.65 and 0.92ppm [see 5-cholanic acid above, Mandava et al. Steroids 23 357 1974]. [Stoll et al. Helv Chim Acta 18 644 1935, Huang-Minlon J Am Chem Soc 7 1 330 1949, Beilstein 9 III 2656, 9 IV 1992.]

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