N-(2-Bromoethyl)phthalimide

Basic information Safety Related Supplier

N-(2-Bromoethyl)phthalimide Basic information

Product Name:
N-(2-Bromoethyl)phthalimide
CAS:
574-98-1
MF:
C10H8BrNO2
MW:
254.08
EINECS:
209-379-9
Mol File:
574-98-1.mol
More
Less

N-(2-Bromoethyl)phthalimide Chemical Properties

Melting point:
80-83 °C(lit.)
Boiling point:
318 °C
Density 
1.6254 (rough estimate)
refractive index 
1.6320 (estimate)
storage temp. 
Store below +30°C.
pka
-2.35±0.20(Predicted)
form 
Crystalline Powder
color 
White to slightly pink or beige
Water Solubility 
insoluble
BRN 
148736
CAS DataBase Reference
574-98-1(CAS DataBase Reference)
NIST Chemistry Reference
N-(beta-bromoethyl)phthalimide(574-98-1)
EPA Substance Registry System
1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethyl)- (574-98-1)
More
Less

Safety Information

Risk Statements 
36/37/38
Safety Statements 
24/25
WGK Germany 
3
TSCA 
Yes
HS Code 
29251995

MSDS

More
Less

N-(2-Bromoethyl)phthalimide Usage And Synthesis

Chemical Properties

white powder

Purification Methods

The following is to be carried out in an efficient FUME HOOD. Dissolve the compound (180g) in CS2 (500 mL) by refluxing for 15minutes (to cause the separation of the most likely impurity, 1,2-diphthalimidoethane), filter and evaporate under reduced pressure. The product forms light tan crystals (m 78-80o). Recrystallise it from EtOH (charcoal) [the compound (50g) is dissolved in hot 75% EtOH (200mL), boiled for ca 10 minutes, carbon is added (5g, Norite), filter and cool to 0o], to give white crystals (40g) which can be recrystallised (m 80-81o); and further recrystallisation gives m 82-83o. [Salzberg & Supniewski Org Synth Coll Vol I 119 1932, Landini & Rolla Synthesis 389 1976, Beilstein 21/10 V 275.]

N-(2-Bromoethyl)phthalimide Preparation Products And Raw materials

Preparation Products

Raw materials

More
Less

N-(2-Bromoethyl)phthalimideSupplierMore

Tianjin heowns Biochemical Technology Co., Ltd. Gold
Tel:
400 638 7771
Email:
sales@heowns.com
J & K SCIENTIFIC LTD.
Tel:
010-82848833- ;010-82848833-
Email:
jkinfo@jkchemical.com;market6@jkchemical.com
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel:
21-61259100-
Email:
sh@meryer.com
Alfa Aesar
Tel:
400-610-6006; 021-67582000
Email:
saleschina@alfa-asia.com
TCI (Shanghai) Development Co., Ltd.
Tel:
021-67121386 / 800-988-0390
Email:
Sales-CN@TCIchemicals.com
Basic information Safety Related Supplier