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4-Chloro-2,6-diaminopyrimidine

Product Name 4-Chloro-2,6-diaminopyrimidine

CAS156-83-2

MFC4H5ClN4

MW144.56

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  • Mass 

    MS-NW-9997          
6-chloro-2,4-pyrimidinediamine
C4H5ClN4            (Mass of molecular ion:    144)


       Source Temperature: 170 °C
   Sample Temperature:  90 °C
   Direct, 75 eV


          18.0       1.9
      28.0       5.7
      38.0       1.4
      39.0       2.8
      40.0       6.8
      41.0       1.9
      42.0       2.4
      43.0      29.9
      53.0       1.2
      55.0       1.1
      62.0       1.3
      65.0       1.1
      66.0       5.2
      67.0      47.8
      68.0       3.1
      74.0       1.6
      89.0       1.3
      92.0       2.9
     109.0      66.3
     110.0       3.9
     116.0       1.8
     117.0       4.4
     119.0       1.4
     128.0       1.5
     144.0     100.0
     145.0       8.2
     146.0      32.6
     147.0       2.6

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C4 H5 Cl N4 0.033 g : 0.5 ml DMSO-d6
    6-chloro-2,4-pyrimidinediamine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A     *1      6.61
      B     *1      6.37
      C             5.717
  

         Hz     ppm     Int.


       2643.19   6.614    162
   2545.41   6.370    199
   2284.79   5.717   1000

in DMSO-d6



KBr disc



nujol mull





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