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Diethyl 2,6-pyridinedicarboxylate

Product Name Diethyl 2,6-pyridinedicarboxylate

CAS15658-60-3

MFC11H13NO4

MW223.23

¹³CNMR

Mass

MS-IW-7565          
diethyl 2,6-pyridinedicarboxylate
C11H13NO4           (Mass of molecular ion:    223)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      27.0       2.4
      29.0       9.2
      39.0       1.0
      50.0       1.7
      51.0       2.5
      52.0       1.3
      52.5       1.7
      66.0       1.8
      76.0       1.7
      77.0       7.4
      78.0       7.4
      79.0       4.1
      94.0       1.2
     104.0       1.0
     105.0      35.5
     106.0       5.7
     122.0       2.1
     123.0      13.4
     124.0       1.7
     150.0      17.0
     151.0     100.0
     152.0       9.8
     178.0       9.6
     179.0      13.9
     180.0       1.5
     223.0       2.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₃ N O₄	0.041 g : 0.5 ml CDCl₃
diethyl 2,6-pyridinedicarboxylate

    Assign.     Shift(ppm)

      A             8.296
      B             8.031
      C             4.499
      D             1.465

     Hz     ppm     Int.

   3319.95   8.308    270
   3312.13   8.288    334
   3217.04   8.050    108
   3209.47   8.031    119
   3208.98   8.030    108
   3201.42   8.011     84
   1808.96   4.527    161
   1801.76   4.509    487
   1794.68   4.491    510
   1787.60   4.473    171
    592.77   1.484    512
    585.69   1.466   1000
    578.49   1.448    528

in CDCl3

KBr disc

nujol mull

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