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DIPHENYLGERMANIUM DICHLORIDE

Product Name DIPHENYLGERMANIUM DICHLORIDE

CAS1613-66-7

MFC12H10Cl2Ge

MW297.75

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  • Mass 

    MS-NW-8641          
dichlorodiphenylgermane
C12H10Cl2Ge         (Mass of molecular ion:    298)


       Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV


          18.0       2.0
      27.0       3.5
      36.0       2.0
      38.0       1.0
      39.0       3.2
      50.0      14.5
      51.0      64.4
      52.0       4.1
      63.0       1.1
      74.0       3.8
      75.0       4.2
      76.0       7.8
      77.0     100.0
      78.0       8.0
      95.0       2.3
      97.0       3.1
      98.0       1.1
      99.0       4.2
     101.0       1.0
     105.0      18.0
     107.0      29.9
     108.0       6.9
     109.0      39.6
     110.0       2.4
     111.0      17.1
     112.0       1.1
     113.0       2.2
     121.0       2.0
     123.0       2.7
     125.0       2.3
     126.0       1.1
     127.0       1.3
     147.0       7.2
     149.0       9.6
     150.0       3.7
     151.0      13.7
     152.0      10.7
     153.0       8.4
     154.0      79.6
     155.0      10.4
     182.0       8.6
     184.0      14.1
     185.0       4.5
     186.0      19.2
     187.0       2.5
     188.0       8.2
     190.0       1.1
     217.0       8.7
     219.0      17.2
     220.0       4.7
     221.0      24.2
     222.0       5.0
     223.0      15.1
     224.0       3.2
     225.0       5.2
     226.0       3.1
     227.0       1.7
     259.0      32.5
     260.0       5.3
     261.0      54.1
     262.0      20.4
     263.0      73.0
     264.0      13.9
     265.0      31.9
     266.0       4.3
     267.0       4.6
     294.0      14.3
     295.0       1.9
     296.0      28.5
     297.0       9.2
     298.0      39.8
     299.0       8.8
     300.0      24.3
     301.0       3.7
     302.0       6.3
     303.0       1.3
     305.0       1.4
     307.0       1.7
     309.0       1.2
     340.0       1.4
     342.0       2.0
     344.0       1.5

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H10 Cl2 Ge ca 10 mg : 0.5 ml CDCl3
    dichlorodiphenylgermane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.67
      B             7.45
      C             7.42
     
     CONFIRMED BY LAOCN PROGRAM
  

         Hz     ppm     Int.


        698.94   7.805     37
    697.44   7.788     50
    694.44   7.754    271
    692.00   7.727    358
    688.56   7.689    544
    687.25   7.674    277
    686.06   7.661    365
    684.81   7.647    528
    682.44   7.620    195
    680.38   7.597    115
    679.69   7.590    114
    678.69   7.579    123
    675.88   7.547     70
    672.25   7.507    161
    670.94   7.492    242
    668.38   7.463   1000
    666.06   7.438    836
    663.44   7.408    433
    663.00   7.403    428
    661.56   7.387    491
    658.88   7.357    210
    658.06   7.348    187
    655.56   7.320     85
    654.94   7.313     81
    653.63   7.299     82
    652.13   7.282     44

in CDCl3



liquid film





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