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2,2'-METHYLENEBIS(4-METHYLPHENOL)

Product Name 2,2'-METHYLENEBIS(4-METHYLPHENOL)

CAS3236-63-3

MFC15H16O2

MW228.29

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  • Mass 

    MS-IW-6461          
2,2'-methylenebis(p-cresol)
C15H16O2            (Mass of molecular ion:    228)


       Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV


          18.0       1.7
      39.0       1.5
      51.0       1.7
      53.0       1.3
      55.0       1.0
      63.0       1.0
      65.0       2.3
      76.0       1.3
      77.0       5.8
      78.0       1.4
      79.0       1.9
      89.0       1.7
      90.0       1.7
      91.0       7.3
      92.0       2.8
      93.0       1.6
      97.0       2.0
      99.0       1.2
     104.0       3.3
     105.0       2.1
     106.0       1.2
     107.0      12.2
     108.0      71.5
     109.0       5.5
     113.0       3.4
     114.0       5.0
     115.0       2.0
     119.0       2.1
     120.0       4.0
     121.0     100.0
     122.0       9.9
     128.0       1.3
     141.0       1.2
     145.0       1.0
     152.0       1.9
     153.0       1.2
     165.0       5.2
     166.0       3.5
     167.0       1.4
     181.0       1.7
     195.0       6.8
     196.0       1.4
     197.0       1.3
     208.0       1.0
     209.0       4.7
     210.0       1.7
     211.0       2.3
     212.0       1.2
     213.0       2.1
     227.0       4.8
     228.0      95.2
     229.0      15.7
     230.0       1.6

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H16 O2 0.038 g : 0.5 ml CDCl3
    2,2'-methylenebis(p-cresol)
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.67
      B             7.070
      C             6.836
      D             6.685
      E             3.837
      F             2.237
  

         Hz     ppm     Int.


       3065.31   7.670    484
   2826.66   7.073    195
   2824.58   7.068    196
   2737.67   6.851     97
   2737.18   6.849     96
   2735.47   6.845     95
   2729.49   6.830    119
   2729.00   6.829    119
   2727.42   6.825    115
   2675.17   6.694    281
   2666.99   6.674    219
   1533.57   3.838    321
    894.04   2.238   1000

in CDCl3



KBr disc



nujol mull



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