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MassMS-NW-0567 2,5-xylidine C8H11N (Mass of molecular ion: 121)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.2 27.0 2.8 28.0 3.3 30.0 1.4 38.0 1.3 39.0 5.6 41.0 2.6 42.0 3.4 50.0 1.9 51.0 4.6 52.0 2.9 53.0 4.5 54.0 1.6 58.5 1.7 59.5 1.7 60.5 1.7 63.0 1.8 65.0 3.8 66.0 1.5 77.0 12.1 78.0 5.8 79.0 4.8 80.0 2.3 91.0 8.0 92.0 2.0 93.0 4.4 94.0 1.5 103.0 4.9 104.0 5.3 105.0 2.3 106.0 53.3 107.0 5.0 118.0 2.3 119.0 1.7 120.0 54.0 121.0 100.0 122.0 9.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.04 ml : 0.5 ml CDCl3 2,5-xylidine 
Assign. Shift(ppm)
A 6.900 B 6.49 C 6.47 D 3.43 E 2.225 F 2.101
Hz ppm Int.622.81 6.955 104 615.19 6.870 156 614.88 6.866 159 585.75 6.541 142 579.13 6.467 403 578.81 6.463 393 307.19 3.430 275 199.69 2.230 951 199.31 2.226 972 188.13 2.101 1000
in CDCl3
CCl4 solution
liquid film
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