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MassMS-NW-8639 tetrabutylgermane C16H36Ge (Mass of molecular ion: 302)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
27.0 2.6 28.0 1.3 29.0 8.6 39.0 1.4 41.0 5.7 55.0 30.4 56.0 1.8 57.0 2.4 70.0 2.3 71.0 1.5 72.0 3.0 73.0 4.5 74.0 4.6 75.0 4.8 76.0 1.4 77.0 3.4 85.0 5.3 87.0 14.2 88.0 2.7 89.0 18.7 90.0 3.4 91.0 14.5 93.0 2.7 99.0 5.3 100.0 1.4 101.0 11.2 102.0 3.1 103.0 13.1 104.0 2.8 105.0 9.1 107.0 1.6 127.0 2.6 128.0 3.0 129.0 42.6 130.0 6.2 131.0 55.8 132.0 20.2 133.0 69.5 134.0 3.8 135.0 14.4 185.0 56.3 186.0 5.6 187.0 74.6 188.0 28.0 189.0 100.0 190.0 8.9 191.0 20.8 192.0 1.8 241.0 18.8 242.0 2.5 243.0 24.8 244.0 10.3 245.0 33.4 246.0 4.4 247.0 7.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H36 Ge 0.05 ml : 0.5 ml CDCl3 tetrabutylgermane 
Assign. Shift(ppm)
A 1.316 B 0.888 C 0.693
Hz ppm Int.545.78 1.366 45 541.87 1.356 75 539.43 1.350 82 535.16 1.340 275 534.06 1.337 231 530.88 1.329 381 527.59 1.321 609 523.32 1.310 516 519.78 1.301 515 516.36 1.293 234 513.55 1.285 125 506.96 1.269 44 371.58 0.930 34 364.75 0.913 108 361.94 0.906 460 359.01 0.899 248 356.45 0.892 354 354.86 0.888 1000 350.95 0.879 256 349.37 0.875 254 347.66 0.870 406 340.70 0.853 30 291.99 0.731 37 290.16 0.727 42 284.91 0.713 294 282.23 0.707 170 280.52 0.702 224 276.73 0.693 341 273.19 0.684 226 268.55 0.672 276
liquid film
4880 A,200 M,liquid
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