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MassMS-NW-5130 1-tetradecene C14H28 (Mass of molecular ion: 196)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 17.5 28.0 1.2 29.0 37.3 36.0 1.3 39.0 16.5 40.0 3.3 41.0 79.8 42.0 22.0 43.0 100.0 44.0 3.4 53.0 6.6 54.0 13.1 55.0 92.2 56.0 78.1 57.0 91.1 58.0 4.2 65.0 1.1 66.0 1.2 67.0 13.0 68.0 14.9 69.0 75.9 70.0 76.3 71.0 36.8 72.0 2.1 79.0 1.1 81.0 5.7 82.0 17.9 83.0 77.7 84.0 44.2 85.0 17.8 86.0 1.2 95.0 1.9 96.0 7.5 97.0 54.5 98.0 24.3 99.0 3.4 110.0 3.6 111.0 23.9 112.0 14.9 113.0 1.9 124.0 1.7 125.0 10.0 126.0 9.0 127.0 1.2 139.0 3.0 140.0 3.7 153.0 1.4 154.0 3.4 168.0 3.5 196.0 4.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H28 0.04 ml : 0.5 ml CDCl3 1-tetradecene 
Assign. Shift(ppm)
A 5.79 B 4.98 C 4.92 D 2.02 E 1.26 F 0.89
Hz ppm Int.453.25 5.061 44 446.44 4.985 39 445.19 4.971 30 436.44 4.874 47 435.25 4.860 33 179.38 2.003 31 179.19 2.001 31 113.06 1.263 1000 84.13 0.940 39 82.44 0.921 32 80.94 0.904 32 78.88 0.881 109
in CDCl3
liquid film
4880 A,200 M,liquid
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