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氯代磷酸双(2,4-二氯苯基)酯

产品名称 氯代磷酸双(2,4-二氯苯基)酯

CAS号14254-41-2

分子式C12H6Cl5O3P

分子量406.41

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  • Mass

    MS-IW-9442          
    bis(2,4-dichlorophenyl) phosphorochloridate
    C12H6Cl5O3P         (Mass of molecular ion:    404)
    

       Source Temperature: 160 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          18.0       2.3
          28.0       4.8
          35.0       4.6
          36.0      45.8
          37.0       3.3
          38.0      16.4
          39.0       1.4
          47.0      18.5
          49.0       2.1
          50.0       4.8
          51.0       2.4
          53.0       2.0
          61.0       4.1
          62.0      11.2
          63.0      36.7
          64.0       2.0
          72.0       4.1
          73.0      22.2
          74.0      14.6
          75.0      17.5
          76.0       1.0
          79.0       3.2
          83.0       7.6
          84.0       3.5
          85.0       6.9
          86.0       1.6
          87.0       1.7
          96.0       1.0
          97.0       8.7
          98.0       8.0
          99.0       4.5
         100.0       2.5
         101.0       2.1
         103.0       1.1
         107.0       5.4
         108.0       1.4
         109.0      23.6
         110.0       5.1
         111.0       7.6
         112.0       1.6
         126.0       7.7
         128.0       2.5
         133.0      57.7
         134.0       3.8
         135.0      36.8
         136.0       2.3
         137.0       6.6
         145.0      13.9
         146.0       1.6
         147.0       8.9
         149.0       1.7
         161.0     100.0
         162.0      13.4
         163.0      64.2
         164.0       8.2
         165.0      10.9
         166.0       1.4
         173.0      15.8
         174.0       1.2
         175.0       5.4
         180.0       1.2
         182.0       1.2
         189.0       3.8
         191.0       1.3
         202.0       1.8
         203.0       2.8
         204.0       1.8
         207.0       2.0
         208.0       8.9
         209.0       1.9
         210.0       5.7
         212.0       1.0
         224.0       1.9
         225.0       1.6
         226.0       1.3
         227.0       5.5
         229.0       4.6
         231.0       1.5
         235.0       1.0
         236.0       9.5
         237.0       1.9
         238.0       6.4
         240.0       1.1
         243.0      19.6
         244.0       1.5
         245.0      18.4
         246.0       1.3
         247.0       5.9
         252.0       1.1
         270.0       4.0
         271.0       3.2
         272.0       4.1
         273.0       3.1
         274.0       1.7
         275.0       1.0
         306.0       1.3
         308.0       1.6
         369.0      75.1
         370.0       3.9
         371.0      92.2
         372.0      13.5
         373.0      45.7
         374.0       6.4
         375.0      10.0
         376.0       1.4
         377.0       1.0
         404.0      17.5
         406.0      26.5
         407.0       2.3
         408.0      16.8
         409.0       2.5
         410.0       5.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H6 Cl5 O3 P 0.039 g : 0.5 CDCl3
    bis(2,4-dichlorophenyl) phosphorochloridate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.501 B 7.496 C 7.300

         Hz     ppm     Int.
    

       3007.20   7.525     25
       3005.49   7.521     34
       3001.34   7.510    511
       2999.63   7.506   1000
       2998.41   7.503    595
       2997.31   7.500    592
       2995.97   7.497    556
       2992.43   7.488    562
       2990.72   7.484    564
       2922.85   7.314    427
       2922.36   7.313    405
       2920.29   7.308    382
       2919.80   7.306    370
       2914.06   7.292    341
       2913.45   7.291    332
       2911.50   7.286    317
       2911.01   7.284    295
    

in CDCl3



KBr disc



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