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碳酸叔丁基-2,4,5-三氯苯酯

产品名称 碳酸叔丁基-2,4,5-三氯苯酯

CAS号16965-08-5

分子式C11H11Cl3O3

分子量297.56

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  • Mass

    MS-IW-2322          
    tert-butyl 2,4,5-trichlorophenyl carbonate
    C11H11Cl3O3         (Mass of molecular ion:    296)
    

       Source Temperature: 180 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          26.0       1.1
          27.0       6.1
          28.0       5.9
          29.0      13.0
          36.0       1.7
          37.0       2.9
          38.0       2.9
          39.0      18.6
          40.0       4.5
          41.0      61.9
          42.0       3.2
          43.0       4.4
          44.0      36.3
          45.0       6.0
          48.0       3.5
          49.0       2.6
          50.0       3.3
          51.0       2.4
          53.0       4.6
          54.0       1.1
          55.0      10.5
          56.0      26.2
          57.0     100.0
          58.0       6.2
          59.0       1.6
          60.0       1.5
          61.0       5.6
          62.0       8.6
          63.0       3.5
          66.0       2.2
          67.0       1.2
          72.0       2.9
          73.0       4.9
          74.0       2.8
          75.0       1.3
          80.0       1.3
          83.0       2.8
          84.0       1.4
          85.0       1.9
          91.0       1.3
          96.0       2.5
          97.0      26.8
          98.0       4.6
          99.0      10.7
         100.0       1.5
         107.0       4.8
         108.0       1.5
         109.0       4.5
         111.0       1.0
         132.0      17.3
         133.0       9.5
         134.0      11.4
         135.0       5.8
         136.0       2.1
         143.0       2.1
         144.0       1.7
         145.0       1.5
         146.0       1.0
         160.0       3.4
         161.0       1.2
         162.0       3.3
         164.0       1.0
         167.0       5.5
         169.0       5.3
         171.0       1.7
         179.0      12.0
         181.0      11.4
         183.0       3.6
         195.0       1.0
         196.0      81.3
         197.0       6.8
         198.0      78.7
         199.0       5.8
         200.0      25.1
         201.0       1.8
         202.0       2.8
         223.0       9.0
         225.0       8.6
         227.0       2.7
         281.0       3.8
         283.0       3.6
         285.0       1.1
    

parameter in CDCl3


  • 1H NMR 300 MHz
    C11 H11 Cl3 O3 0.043 g : 0.5 ml CDCl3
    tert-butyl 2,4,5-trichlorophenyl carbonate
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 7.542 D(B) 7.354 J(A,B) 0.35 D(C) 1.559

         Hz     ppm     Int.
    

       2262.60   7.542     93
       2206.22   7.354     88
        467.68   1.559   1000
    

in CDCl3



KBr disc