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网站主页CAS数据库列表 17231-95-7更多图谱2,3-二氯苯硫酚(17231-95-7)核磁图(13CNMR)

2,3-二氯苯硫酚

产品名称 2,3-二氯苯硫酚

CAS号17231-95-7

分子式C6H4Cl2S

分子量179.07

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  • Mass

    MS-NW-9419          
    2,3-dichlorobenzenethiol
    C6H4Cl2S            (Mass of molecular ion:    178)
    

       Source Temperature: 250 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          36.0       3.2
          37.0       3.5
          38.0       2.6
          39.0       2.8
          44.0       1.9
          45.0       7.8
          49.0       1.8
          50.0       2.9
          51.0       1.0
          52.5       1.6
          53.0       8.3
          53.5       1.6
          54.0       1.3
          57.0       1.6
          58.0       3.3
          60.0       1.0
          61.0       3.8
          62.0       5.7
          63.0      11.1
          68.0       1.0
          69.0      14.7
          70.0       1.3
          71.0      11.4
          71.5       1.3
          72.0       5.2
          73.0       6.6
          74.0       6.9
          75.0       5.7
          79.0       4.6
          81.0       6.5
          82.0       5.4
          83.0       1.4
          84.0       3.5
          85.0       1.7
          86.0       1.0
          89.0       5.0
          90.0       3.3
          91.0       1.0
          92.0       1.0
          93.0       1.5
          97.0       3.2
          99.0       7.0
         101.0       2.0
         103.0       2.5
         105.0       2.6
         106.0       3.6
         107.0      26.7
         108.0      26.8
         109.0       8.3
         110.0       2.4
         111.0       2.2
         116.0       1.3
         118.0       2.5
         133.0       2.6
         134.0       6.7
         135.0       1.9
         136.0       4.3
         142.0      36.4
         143.0      88.5
         144.0      20.8
         145.0      34.0
         146.0       5.7
         147.0       2.5
         148.0       1.7
         177.0       5.6
         178.0     100.0
         179.0      11.0
         180.0      68.2
         181.0       5.7
         182.0      13.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H4 Cl2 S 0.027 g : 0.5 ml CDCl3
    2,3-dichlorobenzenethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.23 B 7.042 C 4.00

         Hz     ppm     Int.
    

       2895.87   7.247     85
       2894.41   7.243    701
       2893.19   7.240     99
       2891.85   7.236     35
       2890.14   7.232     23
       2886.84   7.224    786
       2886.47   7.223    793
       2821.78   7.061    314
       2814.09   7.042    296
       2813.48   7.040    286
       2805.91   7.021    208
       1600.22   4.005   1000
    

in CDCl3



KBr disc



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