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网站主页CAS数据库列表 19755-53-4更多图谱2-溴-3-硝基吡啶(19755-53-4)核磁图(13CNMR)

2-溴-3-硝基吡啶

产品名称 2-溴-3-硝基吡啶

CAS号19755-53-4

分子式C5H3BrN2O2

分子量202.99

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  • Mass

    MS2015-05170CW      
    2-bromo-3-nitropyridine
    C5H3BrN2O2          (Mass of molecular ion:    202)
    

       Source Temperature: 245 °C
       Sample Temperature:  25 °C
       Direct, 70 eV
    

          26.0       2.4
          30.0       3.6
          37.0       1.9
          38.0       3.2
          39.0       2.5
          49.0       3.2
          50.0      17.6
          51.0      10.6
          52.0       2.5
          64.0       1.5
          65.0       1.0
          75.0       5.0
          76.0      54.9
          77.0      15.6
          79.0       1.0
          81.0       1.0
         105.0       1.5
         106.0       3.6
         107.0       1.5
         108.0       3.4
         128.0       1.6
         129.0       9.0
         130.0       2.9
         131.0       8.7
         132.0       1.4
         144.0       8.8
         146.0       8.6
         156.0     100.0
         157.0       6.0
         158.0      97.8
         159.0       5.6
         202.0      78.9
         203.0       5.1
         204.0      77.9
         205.0       5.1
    

in CDCl3

parameter in acetone




  • 1H NMR 300 MHz
    C5 H3 Br N2 O2 ca 7 wt% in acetone
    2-bromo-3-nitropyridine
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.669 D(B) 7.744 D(C) 8.394 J(A,B) 4.78 J(A,C) 1.70 J(B,C) 8.02 GERIG,J.T. & REINHEIMER,J.D. ORG.MAGN.RESON. 1, 239 (1969)

         Hz     ppm     Int.
    

       2603.97   8.680    913
       2602.28   8.674    957
       2599.19   8.664    954
       2597.50   8.658    980
       2523.14   8.410    918
       2521.44   8.405    888
       2515.12   8.384   1000
       2513.42   8.378    960
       2329.50   7.765    957
       2324.72   7.749    935
       2321.48   7.738    893
       2316.71   7.722    853
    

in CDCl3



KBr disk



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