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网站主页CAS数据库列表 24463-19-2更多图谱9-氯甲基蒽(24463-19-2)质谱(MS)

9-氯甲基蒽

产品名称 9-氯甲基蒽

CAS号24463-19-2

分子式C15H11Cl

分子量226.7

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  • Mass

    MS-NW-7186          
    9-(chloromethyl)anthracene
    C15H11Cl            (Mass of molecular ion:    226)
    

       Source Temperature: 140 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          18.0       2.4
          63.0       2.2
          69.5       1.7
          74.0       1.2
          75.0       1.1
          81.0       1.3
          81.5       3.9
          82.0       1.9
          82.5       8.3
          83.0       1.3
          87.0       1.1
          93.5       3.7
          94.0       5.2
          94.5      14.9
          95.0       9.8
          95.5       9.4
          96.0       2.0
         113.0       4.4
         113.5       1.0
         114.0       1.5
         139.0       1.3
         152.0       1.2
         163.0       3.7
         164.0       1.6
         165.0       4.9
         176.0       1.1
         187.0       4.3
         188.0       3.5
         189.0      25.2
         190.0       9.2
         191.0     100.0
         192.0      19.4
         193.0       2.0
         225.0       2.1
         226.0      26.0
         227.0       5.3
         228.0       9.1
         229.0       1.6
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C15 H11 Cl 0.037 g : 0.5 ml CDCl3
    9-(chloromethyl)anthracene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.392 B 8.253 C 7.952 D *1 7.56 E *1 7.44 F 5.528

         Hz     ppm     Int.
    

        751.63   8.393    242
        745.06   8.320    119
        744.25   8.311    168
        742.81   8.294    193
        741.94   8.285    162
        740.25   8.266     54
        739.69   8.260     54
        737.56   8.236    119
        735.75   8.216    171
        734.38   8.200    238
        733.44   8.190    153
        730.88   8.161     48
        729.63   8.147     38
        720.94   8.050     31
        717.69   8.014    169
        716.69   8.003    152
        716.06   7.996    135
        714.94   7.983    114
        714.25   7.976    106
        710.25   7.931    262
        708.50   7.911    199
        707.88   7.904    251
        704.50   7.867     37
        703.31   7.853     50
        685.44   7.654    106
        683.69   7.634    152
        682.25   7.618     57
        682.13   7.617     57
        678.94   7.581    337
        677.13   7.561    264
        675.13   7.539    136
        673.31   7.518    316
        671.25   7.495    551
        668.56   7.465    274
        666.81   7.446    142
        665.25   7.428    214
        663.88   7.413    227
        660.88   7.380     41
        658.69   7.355     97
        657.31   7.340     79
        495.13   5.529   1000
        489.38   5.465     31
    


  • 1H NMR 399.65 MHz
    C15 H11 Cl 0.032 g : 0.5 ml CDCl3
    9-(chloromethyl)anthracene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.405 B 8.257 C 7.964 D 7.561 E 7.455 F 5.535 ASSIGNED BY C-H COSY.

         Hz     ppm     Int.
    

       3359.01   8.405    260
       3305.05   8.270    257
       3304.20   8.268    273
       3296.14   8.248    278
       3295.29   8.246    289
       3187.99   7.977    231
       3187.26   7.976    272
       3186.65   7.974    255
       3179.44   7.956    254
       3178.83   7.955    298
       3178.22   7.953    274
       3177.49   7.951    185
       3030.64   7.584    168
       3029.30   7.580    180
       3024.17   7.568    229
       3022.83   7.564    238
       3021.85   7.562    194
       3020.39   7.558    177
       3015.26   7.545    218
       3013.92   7.542    215
       2986.69   7.474    202
       2985.72   7.471    217
       2980.10   7.457    163
       2979.00   7.455    188
       2978.27   7.453    216
       2977.29   7.450    207
       2971.68   7.436    143
       2970.70   7.434    146
       2212.28   5.536   1000
    

in CDCl3



KBr disc



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