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网站主页CAS数据库列表 3817-11-6更多图谱N-丁基-N-(4-羟丁基)亚硝胺(3817-11-6)核磁图(1HNMR)

N-丁基-N-(4-羟丁基)亚硝胺

产品名称 N-丁基-N-(4-羟丁基)亚硝胺

CAS号3817-11-6

分子式C8H18N2O2

分子量174.24

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  • Mass

    MS-NW-1350          
    4-(n-butyl-N-nitrosoamino)-1-butanol
    C8H18N2O2           (Mass of molecular ion:    174)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       5.2
          17.0       1.2
          18.0       6.0
          19.0       1.4
          26.0       2.0
          27.0      25.5
          28.0      18.3
          29.0      50.4
          30.0      49.5
          31.0      38.9
          32.0       1.5
          39.0      13.4
          40.0       2.2
          41.0      61.1
          42.0      57.5
          43.0      85.4
          44.0      55.7
          45.0       5.5
          47.0       1.0
          53.0       3.3
          54.0       4.4
          55.0     100.0
          56.0      23.3
          57.0      68.8
          58.0       7.3
          59.0       2.7
          60.0       1.9
          67.0       1.5
          68.0       3.9
          69.0       3.0
          70.0      27.8
          71.0      41.8
          72.0      13.5
          73.0      13.5
          74.0       3.8
          81.0       1.6
          82.0       6.2
          83.0       2.6
          84.0      73.3
          85.0       8.6
          86.0      11.5
          87.0       2.0
          95.0       2.1
          97.0       1.5
          98.0       2.5
          99.0       5.6
         100.0      27.5
         101.0      10.9
         102.0      13.2
         103.0       3.9
         114.0       1.8
         115.0      15.1
         116.0       2.8
         125.0       1.3
         126.0      11.6
         127.0       2.0
         128.0       1.0
         129.0       1.0
         130.0       1.2
         131.0       1.3
         132.0       1.7
         143.0       2.4
         144.0       4.8
         157.0      42.8
         158.0       4.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H18 N2 O2 0.04 ml : 0.5 ml CDCl3
    4-(N-butyl-N-nitrosoamino)-1-butanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.11 B 4.09 C 3.68 D 3.63 E 3.59 F 3.56 G 2.57 J 2.10 to 1.08 K 0.97 L 0.92

         Hz     ppm     Int.
    

        375.50   4.193    147
        373.13   4.167    194
        368.63   4.117    329
        366.19   4.089    312
        361.56   4.038    197
        358.94   4.008    214
        336.50   3.758    203
        330.38   3.689    470
        328.31   3.666    177
        327.44   3.657    154
        325.69   3.637    491
        324.50   3.624    386
        321.06   3.585    286
        319.94   3.573    268
        318.81   3.560    251
        313.63   3.502    128
        310.94   3.472    170
        230.19   2.571    885
        176.81   1.975    135
        175.00   1.954    121
        174.44   1.948    125
        173.44   1.937     98
        172.56   1.927    156
        172.13   1.922    154
        171.38   1.914    135
        170.63   1.906    161
        169.56   1.894    189
        168.56   1.883    215
        166.88   1.864    203
        165.19   1.845    296
        162.00   1.809    315
        160.19   1.789    284
        156.50   1.748    372
        155.44   1.736    355
        154.63   1.727    329
        154.31   1.723    327
        152.75   1.706    245
        150.19   1.677    480
        146.25   1.633    364
        145.50   1.625    404
        144.00   1.608    446
        142.19   1.588    776
        140.38   1.568    563
        139.06   1.553    621
        135.50   1.513    709
        132.50   1.480    362
        129.56   1.447    407
        127.69   1.426    341
        126.44   1.412    393
        124.44   1.390    334
        123.25   1.377    286
        122.06   1.363    388
        119.69   1.337    382
        117.38   1.311    230
        116.25   1.299    159
        115.38   1.289    127
        114.94   1.284    126
        113.06   1.263    270
        112.25   1.254    229
        110.88   1.239    168
        106.88   1.194    102
        105.19   1.175    109
        104.75   1.170    107
        104.25   1.165    108
         93.19   1.041    465
         86.81   0.970   1000
         81.81   0.914    877
         79.50   0.888    451
         77.44   0.865    272
         74.44   0.832    203
         72.19   0.807    116
         71.38   0.798    103
    

CCl4 solution



liquid film