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网站主页CAS数据库列表 41492-05-1更多图谱对丁基溴苯(41492-05-1)质谱(MS)

对丁基溴苯

产品名称 对丁基溴苯

CAS号41492-05-1

分子式C10H13Br

分子量213.11

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  • Mass

    MS-IW-9540          
    1-bromo-4-butylbenzene
    C10H13Br            (Mass of molecular ion:    212)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       5.1
          29.0       2.2
          38.0       1.0
          39.0       6.0
          41.0       4.4
          43.0       3.8
          50.0       3.9
          51.0       6.2
          52.0       1.2
          57.5       1.1
          58.0       1.2
          62.0       1.6
          63.0       6.0
          64.0       2.6
          65.0       3.0
          74.0       1.5
          75.0       3.0
          76.0       2.5
          77.0       8.7
          78.0       3.2
          89.0      12.1
          90.0      20.6
          91.0      32.3
          92.0       2.5
         102.0       2.4
         103.0       5.2
         104.0       7.9
         105.0       2.5
         115.0       2.4
         116.0       1.7
         117.0       1.3
         133.0       4.5
         156.0       1.6
         158.0       1.6
         169.0     100.0
         170.0      14.2
         171.0      97.6
         172.0      13.9
         183.0       1.1
         185.0       1.0
         212.0      25.0
         213.0       2.8
         214.0      24.4
         215.0       2.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H13 Br 0.05 ml : 0.5 ml CDCl3
    1-bromo-4-butylbenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.359 B 7.019 C 2.532 D 1.548 E 1.320 F 0.887

         Hz     ppm     Int.
    

       2948.12   7.377    107
       2945.56   7.371    537
       2943.85   7.367    199
       2939.09   7.355    224
       2937.38   7.350    573
       2934.81   7.344     87
       2811.28   7.035    115
       2808.84   7.029    503
       2802.25   7.012    193
       2800.54   7.008    424
       2800.17   7.007    407
       1019.78   2.552    268
       1012.08   2.533    360
       1004.27   2.513    277
        634.16   1.587     90
        627.93   1.572    137
        626.71   1.569    179
        624.76   1.564    121
        620.85   1.554    151
        619.02   1.549    297
        616.21   1.542    131
        612.43   1.533    149
        611.33   1.530    201
        603.64   1.511    107
        545.90   1.366     59
        538.57   1.348    178
        531.13   1.329    254
        523.44   1.310    249
        516.11   1.292    161
        508.79   1.274     50
        376.10   0.942     30
        375.85   0.941     30
        375.12   0.939     30
        369.38   0.925    584
        366.58   0.918     71
        362.06   0.906   1000
        354.74   0.888    490
    

in CDCl3



liquid film