图谱信息 供应商 相关产品
网站主页CAS数据库列表 4350-41-8更多图谱2-对氯苄基吡啶(4350-41-8)质谱(MS)

2-对氯苄基吡啶

产品名称 2-对氯苄基吡啶

CAS号4350-41-8

分子式C12H10ClN

分子量203.67

展开


  • Mass

    MS-NW-5829          
    2-(p-chlorobenzyl)pyridine
    C12H10ClN           (Mass of molecular ion:    203)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       1.2
          27.0       1.8
          28.0       1.2
          38.0       1.2
          39.0       4.5
          50.0       3.1
          51.0       6.2
          52.0       2.1
          62.0       1.7
          63.0       5.1
          64.0       1.2
          65.0       2.6
          69.5       1.0
          70.5       3.3
          73.0       1.1
          74.0       1.3
          75.0       2.7
          77.0       1.0
          78.0       3.5
          82.5       1.4
          83.5      13.6
          84.0       2.2
          87.0       1.0
          89.0       6.5
          90.0       2.2
          99.0       2.2
         101.0       1.1
         111.0       1.2
         113.0       1.1
         114.0       1.1
         115.0       1.9
         125.0       7.5
         126.0       1.0
         127.0       2.7
         139.0       4.3
         140.0       2.6
         141.0       1.7
         165.0       1.2
         166.0       6.3
         167.0      56.0
         168.0      16.9
         169.0       2.7
         189.0       1.4
         201.0       2.8
         202.0     100.0
         203.0      40.9
         204.0      36.7
         205.0      13.2
         206.0       1.6
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H10 Cl N 0.05 ml : 0.5 ml CDCl3
    2-(p-chlorobenzyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.52 B 7.539 C 7.232 D 7.173 E 7.08 F 7.07 G 4.091

         Hz     ppm     Int.
    

       3409.42   8.532    157
       3404.66   8.520    153
       3022.22   7.563    130
       3020.26   7.558    140
       3014.40   7.543    251
       3012.57   7.539    275
       3006.84   7.524    152
       3005.00   7.520    157
       2900.63   7.258     33
       2898.19   7.252     91
       2895.87   7.247    448
       2893.80   7.241    222
       2889.40   7.230    251
       2887.33   7.225    842
       2885.01   7.219    214
       2881.10   7.210     41
       2878.30   7.203     34
       2876.10   7.197     46
       2872.19   7.187    142
       2871.58   7.186    132
       2870.00   7.182    657
       2867.68   7.176    259
       2863.40   7.165    148
       2861.82   7.161    314
       2861.21   7.160    396
       2836.18   7.097    115
       2834.96   7.094    174
       2830.20   7.082    354
       2829.10   7.079    379
       2822.51   7.063    286
       2821.41   7.060    290
       1635.01   4.092   1000
    


  • 1H NMR 89.56 MHz
    C12 H10 Cl N 0.04 ml : 0.5 ml CDCl3
    2-(p-chlorobenzyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.53 B 7.55 C 7.33 to 7.00 D 4.103

         Hz     ppm     Int.
    

        767.88   8.574     93
        766.00   8.553    119
        765.19   8.544     85
        764.13   8.533     60
        762.13   8.510    117
        761.06   8.498     89
        760.25   8.489     91
        686.06   7.661     63
        684.19   7.640     65
        678.44   7.576    158
        677.25   7.562     92
        675.88   7.547     96
        670.88   7.491    129
        668.94   7.470    128
        655.63   7.321     57
        655.25   7.317     56
        654.44   7.308     59
        652.25   7.283     44
        650.75   7.267     54
        649.56   7.253     65
        646.56   7.220   1000
        645.69   7.210    703
        644.88   7.201    820
        641.81   7.167    112
        640.88   7.156    164
        638.38   7.128    162
        636.94   7.112    316
        636.50   7.107    295
        634.50   7.085     89
        633.19   7.071     88
        630.81   7.044     89
        629.50   7.029    190
        628.69   7.020    155
        367.44   4.103    736
    

in CDCl3



liquid film