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2,3'-联吡啶

产品名称 2,3'-联吡啶

CAS号581-50-0

分子式C10H8N2

分子量156.18

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  • Mass

    MS-NW-7293          
    2,3'-bipyridine
    C10H8N2             (Mass of molecular ion:    156)
    

       Source Temperature: 200 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          26.0       1.1
          27.0       1.2
          38.0       1.2
          39.0       2.0
          50.0       7.6
          51.0      11.9
          52.0       5.8
          53.0       1.0
          62.0       1.4
          63.0       2.1
          64.0       2.3
          64.5       2.9
          65.0       1.1
          74.0       2.9
          75.0       4.2
          76.0       5.2
          77.0       4.3
          78.0      16.5
          79.0      10.3
         101.0       3.1
         102.0       3.3
         103.0       2.4
         104.0       9.8
         105.0       1.2
         128.0      10.3
         129.0       6.4
         130.0      21.9
         131.0       2.4
         155.0      68.7
         156.0     100.0
         157.0      11.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H8 N2 0.05 ml : 0.5 ml CDCl3
    2,3'-bipyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.208 B 8.686 C 8.628 D 8.287 E 7.726 F 7.702 G 7.361 J 7.240

         Hz     ppm     Int.
    

       3681.49   9.212    668
       3680.88   9.211    679
       3679.35   9.207    661
       3475.49   8.697    497
       3474.43   8.694    542
       3473.66   8.692    557
       3472.75   8.690    471
       3470.61   8.685    499
       3469.54   8.682    555
       3468.93   8.680    566
       3467.86   8.678    454
       3451.69   8.637    516
       3450.01   8.633    523
       3446.81   8.625    528
       3445.28   8.621    502
       3318.02   8.303    483
       3316.35   8.299    558
       3315.73   8.297    526
       3314.06   8.293    444
       3310.09   8.283    500
       3308.41   8.279    557
       3307.80   8.277    541
       3306.12   8.273    434
       3098.60   7.754    272
       3096.77   7.749    242
       3091.58   7.736    310
       3090.67   7.734    715
       3089.90   7.732    346
       3088.84   7.729    663
       3083.65   7.716    847
       3081.97   7.712   1000
       3081.36   7.711    874
       3080.29   7.708    895
       3079.68   7.706    931
       3078.61   7.704    791
       3073.27   7.690    302
       3072.36   7.688    325
       3071.75   7.687    242
       3070.68   7.684    172
       2948.61   7.378    482
       2947.85   7.377    472
       2943.88   7.367    501
       2942.96   7.364    482
       2940.67   7.359    488
       2939.91   7.357    449
       2935.94   7.347    455
       2935.03   7.345    450
       2900.24   7.257    488
       2898.56   7.253    458
       2895.36   7.245    493
       2893.68   7.241    584
       2893.22   7.240    596
       2891.54   7.236    458
       2888.49   7.228    464
       2886.81   7.224    412
    

in CDCl3



liquid film