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网站主页CAS数据库列表 605-48-1更多图谱9,10-二氯蒽(605-48-1)核磁图(1HNMR)

9,10-二氯蒽

产品名称 9,10-二氯蒽

CAS号605-48-1

分子式C14H8Cl2

分子量247.12

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  • Mass

    MS-NW-2566          
    9,10-dichloroanthracene
    C14H8Cl2            (Mass of molecular ion:    246)
    

       Source Temperature: 200 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          18.0       1.5
          36.0       1.3
          39.0       1.2
          50.0       1.9
          51.0       1.6
          61.0       1.9
          62.0       2.7
          63.0       2.2
          73.0       1.4
          74.0       6.1
          75.0       6.4
          76.0       1.2
          85.0       1.6
          86.0       2.7
          87.0      11.2
          88.0      12.5
          92.0       1.5
          93.0       1.9
          98.0       4.3
          99.0       3.1
         100.0       1.0
         105.0       6.5
         106.0       2.1
         110.0       4.8
         111.0       3.2
         122.0       2.1
         123.0      13.1
         124.0       7.7
         125.0       1.9
         126.0       1.5
         149.0       4.8
         150.0       7.8
         151.0       1.3
         173.0       1.3
         174.0      15.0
         175.0      18.2
         176.0      79.0
         177.0      11.6
         210.0       8.4
         211.0       8.6
         212.0       4.0
         213.0       2.8
         246.0     100.0
         247.0      15.4
         248.0      62.0
         249.0       9.3
         250.0      10.5
         251.0       1.4
    

parameter in CDCl3


  • 1H NMR 300 MHz
    C14 H8 Cl2 in CDCl3
    9,10-dichloroanthracene
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.55 D(B) 7.64 J(A,A') 0.5 J(A,B) 8.9 J(A,B') 1.1 J(A',B) 1.1 J(A',B') 8.9 J(B,B') 8.0 SHARPLESS,N.E. ET AL. ORG.MAGN.RESON. 6, 115 (1974)

         Hz     ppm     Int.
    

       2575.08   8.584     77
       2574.23   8.581     88
       2570.08   8.567    931
       2566.66   8.556    814
       2563.49   8.545    807
       2560.08   8.534   1000
       2555.88   8.520    102
       2555.11   8.517     90
       2301.90   7.673     90
       2301.13   7.670    102
       2296.93   7.656   1000
       2293.52   7.645    807
       2290.35   7.634    814
       2286.93   7.623    931
       2282.78   7.609     88
       2281.93   7.606     77
    

CCl4 solution



KBr disc



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