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网站主页CAS数据库列表 61832-41-5更多图谱N-甲基-1-甲硫基-2-硝基乙烯胺(61832-41-5)红外图谱(IR2)

N-甲基-1-甲硫基-2-硝基乙烯胺

产品名称 N-甲基-1-甲硫基-2-硝基乙烯胺

CAS号61832-41-5

分子式C4H8N2O2S

分子量148.18


  • Mass

    MS-KW-0596          
    N-methyl-1-methylthio-2-nitrovinylamine
    C4H8N2O2S           (Mass of molecular ion:    148)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       6.9
          17.0       1.1
          18.0       5.6
          26.0       1.8
          27.0       8.9
          28.0       6.8
          29.0       2.4
          30.0       6.8
          31.0       1.2
          35.0       3.2
          39.0       1.3
          40.0       2.9
          41.0       4.6
          42.0      17.2
          43.0       3.1
          44.0       7.5
          45.0      17.7
          46.0       5.0
          47.0      12.4
          48.0       7.2
          49.0       1.3
          52.0       2.5
          53.0       1.9
          54.0      19.6
          55.0     100.0
          56.0      18.7
          57.0       5.9
          58.0      17.3
          59.0       2.1
          60.0       1.7
          61.0      18.6
          63.0       1.0
          67.0       6.1
          69.0       1.0
          70.0       2.0
          71.0       9.0
          72.0       6.4
          73.0       5.1
          74.0       6.4
          83.0       1.8
          84.0      16.3
          85.0       8.2
          86.0       7.3
          87.0       6.5
          88.0      15.9
          89.0       1.4
         100.0       2.0
         101.0      77.6
         102.0      10.2
         103.0       1.1
         115.0       1.0
         148.0      16.8
         149.0       1.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C4H8N2O2S 0.040 g : 0.5 ml CDCl3
    N-methyl-1-methylthio-2-nitrovinylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.5 B 6.616 C 3.146 D 2.468 double bond structure is uncertain

         Hz     ppm     Int.
    

       4199.68  10.505     14
       2740.18   6.855      2
       2644.66   6.616    305
       2547.46   6.373      2
       1976.17   4.944      0
       1554.42   3.889      2
       1329.05   3.325      4
       1323.70   3.312      4
       1260.08   3.152    599
       1254.74   3.139    577
       1204.23   3.013      1
       1199.04   3.000      1
       1189.12   2.975      3
       1183.78   2.962      4
       1056.98   2.644      6
       1014.56   2.538      1
        986.49   2.468   1000
        975.19   2.440      4
        914.31   2.288      6
         58.60   0.147      1
    

in CDCl3



KBr disk



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