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N,N-二苄基羟胺

产品名称 N,N-二苄基羟胺

CAS号621-07-8

分子式C14H15NO

分子量213.27

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  • Mass

    MS-IW-0794          
    N,N-dibenzylhydroxylamine
    C14H15NO            (Mass of molecular ion:    213)
    

       Source Temperature: 130 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          18.0       2.3
          39.0       2.0
          51.0       2.1
          63.0       1.4
          65.0       9.7
          77.0       2.8
          89.0       2.6
          90.0       1.8
          91.0     100.0
          92.0      18.6
          93.0       1.1
         104.0       1.9
         105.0       1.8
         106.0      13.8
         107.0       1.2
         117.0       2.3
         118.0       2.0
         120.0       1.6
         122.0       2.2
         168.0       1.0
         181.0       1.2
         194.0       7.2
         195.0       9.5
         196.0       3.8
         197.0       3.4
         211.0       2.1
         213.0      18.5
         214.0       3.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H15 N O 0.033 g : 0.5 ml CDCl3
    N,N-dibenzylhydroxylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.30 to 7.25 B 7.03 C 3.631

         Hz     ppm     Int.
    

       2925.17   7.320    139
       2923.95   7.317    197
       2922.36   7.313    118
       2917.97   7.302    366
       2916.87   7.299    505
       2915.53   7.296    433
       2912.35   7.288    290
       2909.91   7.282    786
       2903.32   7.265   1000
       2900.02   7.257    478
       2898.80   7.254    431
       2896.61   7.248    505
       2894.78   7.244    337
       2891.72   7.236    365
       2888.55   7.228    117
       2886.72   7.224    167
       2885.01   7.219    123
       2883.30   7.215     72
       2808.84   7.029    287
       1451.29   3.632    814
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,liquid