图谱信息 供应商 相关产品
网站主页CAS数据库列表 6484-25-9更多图谱4-氯-2-苯基喹唑啉(6484-25-9)质谱(MS)

4-氯-2-苯基喹唑啉

产品名称 4-氯-2-苯基喹唑啉

CAS号6484-25-9

分子式C14H9ClN2

分子量240.69

展开


  • Mass

    MS-NW-7040          
    4-chloro-2-phenylquinazoline
    C14H9ClN2           (Mass of molecular ion:    240)
    

       Source Temperature: 190 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          18.0       4.1
          27.0       1.2
          39.5       1.7
          50.0       4.8
          51.0       9.4
          52.0       1.8
          63.0       1.4
          74.0       1.7
          75.0       8.8
          76.0       8.3
          77.0      19.1
          78.0       1.5
          89.0       1.0
         100.0       1.0
         102.0      19.8
         102.5       1.6
         103.0       5.0
         104.0       3.0
         119.0       2.3
         120.0       5.6
         120.5       1.1
         121.0       1.9
         151.0       1.7
         177.0       2.0
         205.0     100.0
         206.0      16.0
         207.0       1.3
         222.0       1.8
         240.0      39.6
         241.0       6.6
         242.0      13.4
         243.0       2.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H9 Cl N2 0.042 g : 0.5 ml CDCl3
    4-chloro-2-phenylquinazoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.575 B 8.194 C 8.049 D 7.879 E 7.604 F 7.51

         Hz     ppm     Int.
    

       3436.28   8.599     39
       3431.70   8.587    387
       3430.79   8.585    300
       3429.57   8.582    276
       3427.43   8.577    431
       3424.22   8.569    474
       3421.94   8.563    437
       3418.43   8.554     75
       3279.42   8.206    283
       3278.66   8.204    289
       3274.99   8.195     36
       3271.18   8.186    308
       3270.42   8.184    310
       3221.59   8.062    304
       3213.20   8.041    382
       3157.20   7.900    185
       3155.82   7.897    190
       3150.33   7.883    233
       3148.80   7.879    339
       3147.43   7.876    185
       3141.78   7.862    176
       3140.41   7.858    170
       3046.88   7.624    203
       3045.81   7.622    214
       3039.86   7.607    216
       3038.64   7.604    343
       3037.57   7.601    231
       3031.62   7.586    177
       3030.55   7.584    178
       3014.37   7.543     42
       3013.31   7.540     40
       3012.70   7.539     38
       3008.42   7.528    170
       3006.90   7.524    188
       3004.91   7.519    574
       3003.69   7.516    574
       3000.34   7.508    882
       2997.89   7.502   1000
       2994.23   7.493    140
       2990.88   7.484     40
    

in CDCl3



KBr disc



nujol mull