图谱信息 供应商 相关产品
网站主页CAS数据库列表 7051-16-3更多图谱1-氯-3,5-二甲氧基苯(7051-16-3)质谱(MS)

1-氯-3,5-二甲氧基苯

产品名称 1-氯-3,5-二甲氧基苯

CAS号7051-16-3

分子式C8H9ClO2

分子量172.61

展开


  • Mass

    MS-IW-3609          
    1-chloro-3,5-dimethoxybenzene
    C8H9ClO2            (Mass of molecular ion:    172)
    

       Source Temperature: 220 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          15.0       2.0
          28.0       1.3
          37.0       1.3
          38.0       2.9
          39.0       2.9
          50.0       3.9
          51.0       8.3
          52.0       1.1
          53.0       1.8
          59.0       1.0
          61.0       2.5
          62.0       5.8
          63.0      17.4
          64.0       2.8
          65.0       9.8
          66.0       2.7
          69.0       5.0
          73.0       3.0
          74.0       2.6
          75.0       4.3
          77.0      15.5
          78.0       2.1
          79.0      13.7
          86.0       3.7
          87.0       1.1
          88.0       1.0
          91.0       1.9
          92.0       1.6
          93.0       1.0
          94.0       2.1
          98.0       3.4
          99.0      10.8
         100.0       1.9
         101.0       3.9
         107.0       7.5
         108.0      11.4
         109.0       9.8
         110.0       1.0
         111.0       3.0
         112.0      28.3
         113.0       6.2
         114.0      13.2
         115.0       2.0
         116.0       1.4
         122.0       2.5
         126.0       6.0
         127.0       3.9
         128.0       4.1
         129.0      15.1
         130.0       1.6
         131.0       4.7
         137.0       1.0
         141.0       3.9
         142.0      16.1
         143.0      36.3
         144.0       7.9
         145.0      11.5
         146.0       1.3
         171.0       6.1
         172.0     100.0
         173.0      11.0
         174.0      32.8
         175.0       2.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 Cl O2 0.039 g : 0.5 ml CDCl3
    1-chloro-3,5-dimethoxybenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.507 B 6.337 C 3.762

         Hz     ppm     Int.
    

       2601.93   6.511    263
       2599.73   6.506    280
       2535.03   6.344     71
       2532.71   6.338    126
       2530.52   6.332     66
       1503.66   3.763   1000
    

in CDCl3



KBr disc



nujol mull