4,4'-二氨基-3,3'-二甲基联苯基甲烷

产品名称 4,4'-二氨基-3,3'-二甲基联苯基甲烷

CAS号838-88-0

分子式C15H18N2

分子量226.32

¹³CNMR

Mass

MS-IW-2160          
4,4'-methylenebis(2-methylaniline)
C15H18N2            (Mass of molecular ion:    226)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      28.0       1.5
      39.0       1.3
      42.0       1.1
      51.0       1.4
      52.0       1.1
      53.0       1.0
      65.0       1.6
      77.0       5.0
      78.0       1.6
      79.0       1.1
      90.0       1.3
      91.0       4.0
      92.0       1.3
      93.0       1.0
      96.5       1.8
      97.5       2.6
      98.0       4.3
     103.0       1.2
     104.0       4.6
     104.5       3.1
     105.0       5.5
     105.5       8.1
     106.0       3.9
     107.0       4.5
     112.0       1.2
     112.5       1.2
     113.0       7.5
     113.5       1.2
     115.0       1.0
     117.0       1.3
     118.0       4.4
     119.0       5.9
     120.0      23.4
     121.0       2.2
     165.0       1.6
     167.0       1.4
     168.0       1.2
     180.0       2.7
     181.0       1.4
     182.0       1.2
     183.0       1.0
     193.0       2.8
     194.0       5.0
     195.0       8.1
     196.0       3.7
     208.0       3.4
     209.0       6.1
     210.0      17.7
     211.0      53.8
     212.0       8.7
     223.0       1.3
     225.0      47.4
     226.0     100.0
     227.0      16.4
     228.0       1.3
     345.0       2.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₅ H₁₈ N₂	0.035 g : 0.5 ml CDCl₃
4,4'-methylenebis(2-methylaniline)

    Assign.     Shift(ppm)

      A             6.86
      B             6.84
      C             6.577
      D             3.722
      E             3.40
      F             2.106
     
     J(B,C)=7.9HZ

     Hz     ppm     Int.

   2740.23   6.857    205
   2736.57   6.848    120
   2728.64   6.828    113
   2727.05   6.824     90
   2632.32   6.587    209
   2624.39   6.567    182
   1487.43   3.722    292
   1358.28   3.399     51
    841.92   2.107   1000

in CDCl3

KBr disc

nujol mull

更多供应商

4,4'-二氨基-3,3'-二甲基联苯基甲烷(838-88-0)质谱(MS) 相关产品图谱

4,4'-二氨基-3,3'-二甲基联苯基甲烷(838-88-0)核磁图(¹³CNMR) 4,4'-二氨基-3,3'-二甲基联苯基甲烷(838-88-0)质谱(MS) 4,4'-二氨基-3,3'-二甲基联苯基甲烷(838-88-0)核磁图(¹HNMR) 4,4'-二氨基-3,3'-二甲基联苯基甲烷(838-88-0)红外图谱(IR2) 4,4'-二氨基-3,3'-二甲基联苯基甲烷(838-88-0)红外图谱(IR1)

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