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网站主页CAS数据库列表 85-46-1更多图谱1-萘磺酰氯(85-46-1)质谱(MS)

1-萘磺酰氯

产品名称 1-萘磺酰氯

CAS号85-46-1

分子式C10H7ClO2S

分子量226.68

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  • Mass

    MS-NW-1977          
    1-naphthalenesulfonyl chloride
    C10H7ClO2S          (Mass of molecular ion:    226)
    

       Source Temperature: 230 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       3.2
          36.0       2.4
          39.0       1.8
          44.0       1.0
          48.0       5.0
          50.0       3.6
          51.0       5.6
          62.0       2.1
          63.0       7.9
          63.5       5.1
          64.0      10.8
          74.0       4.3
          75.0       6.1
          76.0       3.2
          77.0      10.2
          78.0       1.0
          81.0       1.2
          86.0       1.0
          87.0       2.1
          89.0       1.0
          98.0       1.1
          99.0       1.1
         100.0       1.1
         101.0       6.3
         102.0       1.8
         115.0       6.3
         125.0       1.1
         126.0      13.6
         127.0     100.0
         128.0      25.0
         129.0       2.3
         143.0       3.9
         147.0       2.4
         159.0       1.4
         162.0      32.1
         163.0       3.8
         164.0      10.4
         165.0       1.0
         175.0       3.9
         191.0      16.7
         192.0       1.9
         193.0       1.0
         206.0       2.1
         208.0       2.0
         226.0      29.2
         227.0       3.3
         228.0      11.0
         229.0       1.3
         252.0       1.4
         253.0       1.7
         254.0       1.1
         285.0       1.6
         286.0       5.5
         287.0       1.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H7 Cl O2 S 0.042 g : 0.5 ml CDCl3
    1-naphthalenesulfonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.78 B 8.354 C 8.20 D 8.00 E *1 7.77 F *1 7.71 G 7.59

         Hz     ppm     Int.
    

        792.75   8.852    197
        791.94   8.843    343
        791.13   8.834    267
        790.50   8.827    372
        789.69   8.818    359
        788.19   8.801     47
        787.00   8.788     40
        786.50   8.782     44
        785.25   8.768    189
        784.31   8.758    237
        783.69   8.751    277
        782.88   8.742    425
        782.19   8.734    439
        781.38   8.725    261
        754.50   8.425     41
        753.00   8.408    562
        751.75   8.394    651
        749.19   8.366     47
        748.81   8.361     44
        748.50   8.358     44
        748.06   8.353     46
        745.56   8.325    658
        744.25   8.311    811
        742.00   8.285     56
        738.56   8.247    438
        735.38   8.212     42
        735.00   8.207     46
        734.56   8.202     40
        733.63   8.192     39
        732.88   8.184     48
        731.19   8.165    408
        730.31   8.155    581
        726.00   8.107     39
        721.00   8.051    248
        719.50   8.034    221
        718.06   8.018    198
        716.06   7.996     51
        715.75   7.992     53
        715.31   7.987     54
        713.63   7.969    529
        711.44   7.944    492
        708.44   7.911     44
        707.13   7.896    176
        705.19   7.874    264
        703.44   7.855     46
        702.56   7.845     40
        701.69   7.835     51
        700.13   7.818    618
        698.25   7.797    399
        696.81   7.781    205
        695.75   7.769     77
        694.06   7.750    638
        692.56   7.733    767
        691.81   7.725    802
        689.94   7.704    441
        686.06   7.661   1000
        684.81   7.647    492
        682.44   7.620     59
        681.88   7.614     53
        681.75   7.613     53
        680.94   7.604     40
        680.50   7.599     44
        678.50   7.576    703
        677.75   7.568    745
        675.69   7.545     46
        670.25   7.484    460
    

KBr disc