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网站主页CAS数据库列表 873-69-8更多图谱2-吡啶甲醛肟(873-69-8)红外图谱(IR1)

2-吡啶甲醛肟

产品名称 2-吡啶甲醛肟

CAS号873-69-8

分子式C6H6N2O

分子量122.12

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  • Mass

    MS-NW-1435          
    2-pyridinecarbaldehyde oxime
    C6H6N2O             (Mass of molecular ion:    122)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          17.0       1.2
          18.0       5.2
          26.0       5.5
          27.0       6.2
          28.0       5.7
          30.0       1.0
          37.0       2.9
          38.0       5.3
          39.0      10.2
          40.0       1.3
          41.0       1.1
          44.0       1.8
          49.0       2.4
          50.0      13.7
          51.0      27.8
          52.0      18.3
          53.0       3.2
          62.0       1.5
          63.0       4.2
          64.0       3.8
          65.0      59.2
          66.0       5.3
          67.0       1.6
          75.0       2.9
          76.0       5.8
          77.0      12.8
          78.0      24.0
          79.0      33.7
          80.0       1.9
          91.0       2.4
          92.0      25.0
          93.0       2.0
          95.0       1.3
         103.0       1.2
         104.0      25.7
         105.0       4.3
         121.0       7.5
         122.0     100.0
         123.0       7.5
    

parameter in DMSO-d6


  • 1H NMR 300 MHz
    C6 H6 N2 O 30 % in DMSO
    2-pyridinecarbaldehyde oxime
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.75 D(B) 7.39 D(C) 7.93 D(D) 7.78 J(A,B) 4.9 J(A,C) 1.8 J(A,D) 1.4 J(B,C) 7.7 J(B,D) 1.0 J(C,D) 8.1 D(E) 8.46 D(F) 12.20 BRUEGEL,W. Z.ELEKTROCHEM.BER.BUNSENGES.PHYS.CHEM. 66, 159 (1962)

         Hz     ppm     Int.
    

       3660.02  12.200   1000
       2629.06   8.764    152
       2627.50   8.758    241
       2625.89   8.753    167
       2624.15   8.747    169
       2622.59   8.742    247
       2621.03   8.737    159
       2538.00   8.460   1000
       2388.22   7.961    109
       2386.48   7.955    109
       2380.28   7.934    229
       2378.49   7.928    225
       2372.47   7.908    171
       2370.73   7.902    168
       2338.87   7.796    198
       2337.71   7.792    313
       2336.55   7.788    204
       2330.80   7.769    143
       2329.59   7.765    213
       2328.43   7.761    138
       2223.67   7.412    163
       2222.69   7.409    163
       2218.81   7.396    165
       2217.78   7.393    169
       2216.04   7.387    161
       2215.02   7.383    153
       2211.14   7.370    147
       2210.15   7.367    144
    

KBr disc



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