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网站主页CAS数据库列表 880-09-1更多图谱二哌啶甲烷(880-09-1)质谱(MS)

二哌啶甲烷

产品名称 二哌啶甲烷

CAS号880-09-1

分子式C11H22N2

分子量182.31

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  • Mass

    MS-NW-8910          
    dipiperidinomethane
    C11H22N2            (Mass of molecular ion:    182)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.3
          27.0       3.8
          28.0       9.6
          29.0       9.5
          30.0       9.3
          39.0       3.5
          40.0       1.0
          41.0       9.7
          42.0      15.0
          43.0       9.9
          44.0      12.4
          53.0       1.4
          54.0       1.9
          55.0       8.8
          56.0      13.1
          57.0      11.1
          58.0       1.2
          67.0       2.1
          68.0       2.0
          69.0       2.8
          70.0       6.3
          82.0       1.7
          84.0      35.8
          85.0      19.1
          86.0       1.5
          94.0       1.4
          95.0       1.9
          96.0       3.9
          97.0       8.5
          98.0     100.0
          99.0       8.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C11 H22 N2 0.04 ml : 0.5 ml CDCl3
    dipiperidinomethane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.828 B 2.46 to 2.35 C 1.67 to 1.33 CHEMICALLY EXCHENGING SYSTEM.

         Hz     ppm     Int.
    

        255.31   2.851     35
        253.31   2.829   1000
        251.25   2.806     30
        218.94   2.445    251
        215.88   2.411    419
        210.38   2.350    376
        148.75   1.661     59
        147.94   1.652     54
        147.00   1.642     51
        143.13   1.599    166
        142.19   1.588    155
        133.50   1.491    479
        131.81   1.472    630
        130.63   1.459    448
        125.88   1.406     78
        123.63   1.381     60
        123.13   1.375     61
        120.75   1.349     40
        119.94   1.340     35
        119.50   1.335     36
        118.88   1.328     36
        118.44   1.323     35
    

in CDCl3



liquid film