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网站主页CAS数据库列表 92-69-3更多图谱对羟基联苯(92-69-3)核磁图(13CNMR)

对羟基联苯

产品名称 对羟基联苯

CAS号92-69-3

分子式C12H10O

分子量170.21

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  • Mass

    MS-NW-4439          
    biphenyl-4-ol
    C12H10O             (Mass of molecular ion:    170)
    

       Source Temperature: 240 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          39.0       2.8
          50.0       1.4
          51.0       2.5
          55.0       2.7
          57.5       1.1
          62.0       1.2
          63.0       3.4
          65.0       1.4
          70.0       1.1
          72.0       1.6
          74.0       1.1
          75.0       1.2
          76.0       2.2
          77.0       2.0
          84.0       2.3
          85.0       4.4
          89.0       1.9
         102.0       1.3
         115.0      11.2
         116.0       1.7
         127.0       1.0
         139.0       4.0
         140.0       1.3
         141.0      16.2
         142.0       2.7
         151.0       1.3
         152.0       2.2
         153.0       1.6
         155.0       1.0
         168.0       2.1
         169.0       8.1
         170.0     100.0
         171.0      13.4
         172.0       1.1
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H10 O saturated in CDCl3
    biphenyl-4-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.540 B 7.482 C 7.415 D 7.309 E 6.907 F 4.92

         Hz     ppm     Int.
    

       3018.68   7.554    417
       3017.46   7.551    524
       3015.38   7.546    165
       3012.08   7.537    217
       3011.23   7.535    323
       3010.25   7.533    637
       3009.16   7.530    546
       3007.81   7.527     89
       3007.20   7.525    111
       2997.68   7.501    113
       2994.63   7.494    917
       2992.43   7.488    294
       2988.04   7.477    306
       2985.96   7.472    944
       2982.91   7.464    122
       2972.66   7.439    106
       2971.56   7.436    283
       2970.95   7.434    355
       2969.12   7.430    142
       2963.62   7.416    657
       2962.28   7.413    288
       2957.40   7.400    190
       2955.81   7.396    367
       2928.34   7.328    145
       2927.00   7.324    269
       2925.78   7.321    141
       2921.51   7.311    119
       2919.68   7.306    317
       2917.72   7.301    100
       2913.57   7.291     84
       2912.35   7.288    139
       2767.46   6.925    114
       2764.53   6.918   1000
       2762.33   6.912    300
       2757.93   6.901    296
       2755.86   6.896    874
       2752.81   6.889    110
    


  • 1H NMR 89.56 MHz
    C12 H10 O 0.051 g : 0.5 ml CDCl3
    biphenyl-4-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.51 B 7.47 C 7.41 D 7.27 E 6.89 F 4.80

         Hz     ppm     Int.
    

        682.75   7.624     35
        681.88   7.614     55
        680.75   7.602    129
        680.00   7.593    123
        678.25   7.574    162
        677.94   7.570    160
        677.44   7.565    137
        676.75   7.557    126
        676.06   7.549    166
        675.50   7.543    154
        673.81   7.524    724
        671.69   7.500    624
        670.38   7.486    752
        668.88   7.469    373
        667.25   7.451    328
        665.00   7.426   1000
        664.13   7.416    659
        663.13   7.405    637
        661.13   7.382    238
        659.06   7.359    318
        658.25   7.350    238
        656.56   7.331    359
        655.50   7.320    318
        654.56   7.309    249
        651.69   7.277     86
        651.19   7.271    109
        650.44   7.263    115
        649.50   7.253     47
        645.56   7.209     40
        644.50   7.197     33
        624.13   6.969    103
        621.31   6.938    928
        619.00   6.912    280
        614.69   6.864    221
        612.50   6.839    715
        609.63   6.807     73
        432.31   4.828     42
        429.94   4.801    631
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder