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1-Chlorododecane

Basic information Uses Laboratory Preparation Safety Related Supplier

1-Chlorododecane Basic information

Product Name:
1-Chlorododecane
CAS:
112-52-7
MF:
C12H25Cl
MW:
204.78
EINECS:
203-981-5
Mol File:
112-52-7.mol
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1-Chlorododecane Chemical Properties

Melting point:
-9.3 °C
Boiling point:
260 °C
Density 
0.867 g/mL at 20 °C(lit.)
refractive index 
n20/D 1.443
Flash point:
130 °C
storage temp. 
Store below +30°C.
solubility 
<0.007g/l
form 
Liquid
color 
Clear colorless
Water Solubility 
0.0068 g/L (20 ºC)
FreezingPoint 
-9.3℃
BRN 
635778
InChIKey
YAYNEUUHHLGGAH-UHFFFAOYSA-N
CAS DataBase Reference
112-52-7(CAS DataBase Reference)
NIST Chemistry Reference
Dodecane, 1-chloro-(112-52-7)
EPA Substance Registry System
Dodecane, 1-chloro- (112-52-7)
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Safety Information

Hazard Codes 
Xn,N,Xi
Risk Statements 
40-50/53-38-66
Safety Statements 
24-36/37-60-61-37-46
RIDADR 
UN 3082 9/PG 3
WGK Germany 
3
HazardClass 
9
PackingGroup 
III
HS Code 
29031980
HS Code 
29189090

MSDS

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1-Chlorododecane Usage And Synthesis

Uses

Lauroyl chloride is an important organic intermediate and is widely used in the synthesis of surfactants, and it is also used in the synthesis of rubber scorch retardant, medicine and pesticide.

Laboratory Preparation

500 ml round-bottomed flask fitted with a double surface condenser and charged with 109.5 ml (or 179 grams) of freshly distilled thionyl chloride, and 46.5 grams of n-dodecyl alcohol (lauryl alcohol) are slowly added during 2 hours. When all the n-dodecyl alcohol has been added, the reaction mixture is refluxed for 6 hours. The obtained reaction mixture is distilled and the excess of thionyl chloride passes over below 80° C, followed by a small fraction up to 120° C. Finally, the crude 1-chlorododecane distills at 252-257° C, mainly at 255-257° C. The purified 1-chlorododecane is washed with water, 10% sodium carbonate solution, twice with water and dried with anhydrous calcium chloride. 1-Chlorododecane is additionally purified by distillation through an efficient fractionating column. Pure n-hexyl chloride passes over at 116.5° C/5 mm. The yield is 35 grams

Chemical Properties

Liquid

Uses

Barchlor(R) 12 is used as a chemical intermediate.

Uses

Barchlor(R) 12S is used as a chemical intermediate.

General Description

Clear colorless oily liquid.

Air & Water Reactions

Insoluble in water.

Reactivity Profile

1-Chlorododecane may be incompatible with strong oxidizing and reducing agents. May be incompatible with many amines, nitrides, azo/diazo compounds, alkali metals, and epoxides.

Fire Hazard

1-Chlorododecane is combustible.

1-Chlorododecane Preparation Products And Raw materials

Preparation Products

Raw materials

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1-ChlorododecaneSupplierMore

Yancheng Longshen Chemical Co.,Ltd. Gold
Tel:
0515-88718898-
Email:
3004247793@qq.com;
Wuhan Hongde Yuexin Pharmaceutical Technology Co., Lt Gold
Tel:
027-83855392-
Email:
wuhanfudechem03@sina.com;
Yangzhou Prince Chemical Co., Ltd Gold
Tel:
0514-84248359- ;0514-85083801- ;0514-85083813-
Email:
sales@princechem.com;Jenny1102@princechem.com;faneyio@princechem.com
J & K SCIENTIFIC LTD.
Tel:
010-82848833- ;010-82848833-
Email:
jkinfo@jkchemical.com;market6@jkchemical.com
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel:
21-61259100-
Email:
sh@meryer.com
Basic information Uses Laboratory Preparation Safety Related Supplier