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网站主页CAS数据库列表 1613-66-7更多图谱二苯基二氯化锗(1613-66-7)核磁图(13CNMR)

二苯基二氯化锗

产品名称 二苯基二氯化锗

CAS号1613-66-7

分子式C12H10Cl2Ge

分子量297.75

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  • Mass

    MS-NW-8641          
    dichlorodiphenylgermane
    C12H10Cl2Ge         (Mass of molecular ion:    298)
    

       Source Temperature: 260 °C
       Sample Temperature: 130 °C
       Reservoir, 75 eV
    

          18.0       2.0
          27.0       3.5
          36.0       2.0
          38.0       1.0
          39.0       3.2
          50.0      14.5
          51.0      64.4
          52.0       4.1
          63.0       1.1
          74.0       3.8
          75.0       4.2
          76.0       7.8
          77.0     100.0
          78.0       8.0
          95.0       2.3
          97.0       3.1
          98.0       1.1
          99.0       4.2
         101.0       1.0
         105.0      18.0
         107.0      29.9
         108.0       6.9
         109.0      39.6
         110.0       2.4
         111.0      17.1
         112.0       1.1
         113.0       2.2
         121.0       2.0
         123.0       2.7
         125.0       2.3
         126.0       1.1
         127.0       1.3
         147.0       7.2
         149.0       9.6
         150.0       3.7
         151.0      13.7
         152.0      10.7
         153.0       8.4
         154.0      79.6
         155.0      10.4
         182.0       8.6
         184.0      14.1
         185.0       4.5
         186.0      19.2
         187.0       2.5
         188.0       8.2
         190.0       1.1
         217.0       8.7
         219.0      17.2
         220.0       4.7
         221.0      24.2
         222.0       5.0
         223.0      15.1
         224.0       3.2
         225.0       5.2
         226.0       3.1
         227.0       1.7
         259.0      32.5
         260.0       5.3
         261.0      54.1
         262.0      20.4
         263.0      73.0
         264.0      13.9
         265.0      31.9
         266.0       4.3
         267.0       4.6
         294.0      14.3
         295.0       1.9
         296.0      28.5
         297.0       9.2
         298.0      39.8
         299.0       8.8
         300.0      24.3
         301.0       3.7
         302.0       6.3
         303.0       1.3
         305.0       1.4
         307.0       1.7
         309.0       1.2
         340.0       1.4
         342.0       2.0
         344.0       1.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H10 Cl2 Ge ca 10 mg : 0.5 ml CDCl3
    dichlorodiphenylgermane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.67 B 7.45 C 7.42 CONFIRMED BY LAOCN PROGRAM

         Hz     ppm     Int.
    

        698.94   7.805     37
        697.44   7.788     50
        694.44   7.754    271
        692.00   7.727    358
        688.56   7.689    544
        687.25   7.674    277
        686.06   7.661    365
        684.81   7.647    528
        682.44   7.620    195
        680.38   7.597    115
        679.69   7.590    114
        678.69   7.579    123
        675.88   7.547     70
        672.25   7.507    161
        670.94   7.492    242
        668.38   7.463   1000
        666.06   7.438    836
        663.44   7.408    433
        663.00   7.403    428
        661.56   7.387    491
        658.88   7.357    210
        658.06   7.348    187
        655.56   7.320     85
        654.94   7.313     81
        653.63   7.299     82
        652.13   7.282     44
    

in CDCl3



liquid film